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7.5.4 EXAMPLES OF VARIABLE-PARAMETER KINETIC EXPERIMENTS 7.5.4.1 Variable-Temperature Kinetic Experiments Figure 7 shows a kinetic pro le relative to a VTK experiment concerning the racemization of ( )-adrenaline in acidic aqueous solution [49]. It was obtained polarimetrically following the optical rotation . The modulating function used was T = T0 + t, where T0 = 309.6 K and = 0.001694 K/s, realized by a circulation of water coming from a programmed thermostatted bath. The temperature was read inside the polarimetric cell by a platinum resistor. Temperature and absorbance were automatically acquired by a computer connected to the instruments. The typical sigmoidal shape comes from the relation r = kobs[T(t)]C, that is, the reaction rate is given by the product of two terms: kobs[T(t)], which always increases for the increasing temperature, and C, which decreases continously during the reaction. For this reason the reaction is accelerated in its rst part but after the in ection point the low concentration of C is overwhelming and the reaction decelerates until the rate java code 128 reader Barcode Reader . Free Online Web Application
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